J4 ›› 2002, Vol. 10 ›› Issue (3): 1-6.
• 综述·评述 • 下一篇
李中玺,周丽萍,冯玉怀
L I Zhongxi , ZHOU Liping , FENG Yuhuai
摘要:
简述了分光光度、电化学分析、原子吸收光谱、电感藕合等离子体质谱、发射光谱、X 射线荧光光谱等现代分析仪器法在贵金属分析中的应用,并对各种仪器分析法的分析性能进行了比较;简单介绍了新研发的SK- 800 无色散原子荧光测金仪的主要概况。
中图分类号:
TH83
[1] I A Kovalev ,L V Bogacheva. FIA - FAAS system including on2line solid phase extraction forthe determination of Pd ,Pt ,Rh in alloys and ores [J].Talanta. ,2000 ,52 :39 - 50. [2] Mao X Q ,Chen H W. Coprecipitate concentration with DDTC - Cu for the determination ofsilver by flame atomic absorption spectrometry [J].Microchem. J . ,1998 ,58 (3) :383 - 391. [3] 金泽祥,杨洋,陈文武,等. 流动注射在线萃取-石墨炉原子吸收法测定地质样品中痕量钯 [J] .分析试验室,2000 ,19 (4) :37 - 39. [4] 郑永章.流动注射在线分离富集-石墨炉原子吸收法测定氧化铅中痕量金 [J] .分析试验室,2000 ,19 (4) :22 - 26. [5] J G Sen. Determiation of noble metals in silicate rocks ,oresang metallurgical samples by simultaneous multielement graphite furance atomic absorption spectrometry with zeeman background corrction [J].Talanta ,1993 ,40 (6) :791 - 797. [6] Riitta J uvone , Tuula Lakomaa ,Eeva Kallio. Determination of the platinum group elements andgold in rock samples by nickel sulphide fire assaypreconcentration and ICP - MS measurement ,Geological Survey of Finland [J ] . Special Paper ,1993 ,18 :101 - 105. [7] S Yali , Guan Xi yun ,DuAndao. Determination of platinum group elements by inductively coupled plasmamass spectrometry combined fire assay and tellurium coprecipitation [J]. Spectrochim.Acta. PartB. ,1998 ,53 :1463 - 1467. [8] Amosse J . Separation of platinum group elements and gold in geological materials with selenium and tellurium coprecipitation and determination by ICP - MS [J ] . Geostand. Newsl. ,1998 ,22(1) :93 - 102. [9] 靳新娣,朱和平. 电感耦合等离子体质谱法测定地质样品中铂、钯、钌、铑、铱和金 [J].分析化学, 2001 ,29 (6) :653 - 651. [10] I Jarvis ,M M Totland , K E Jarvis. Assessment of Dowex - 1 - X - 8 - based anion – exchange procedures for the separation and determination of ruthenium , rhodium , palladium , iridium ,platinum and gold in geological samples by inductively coupled plasma mass spectrometry [J].Analyst ,1997 ,122 (1) :19 - 28. [11] C E James ,C R Neal ,J A O’Neil , et al. Quantifying the platinum group elements and gold ingeological samples using cation exchange pretreatment and USN inductively coupled plasmamass [J ] . Chem. Geol. , 1999 , 157 ( 2) : 219 -234. [12] Goedo A G, Dorado M T , Padilla I ,et al. Preconcentration and matrix separation of preciousmetals in geological and related materials usingmetalfixchelamine resin prior to inductivitycoupled plasma mass spectrometry [ J ] . Anal.Chim. Acta , 1997 , 340 (1/ 3) : 31 - 39. [13] Jorge A P , Enzweiler J . Determination of platinum group lements and gold in nickel sulfidefire assay button using an ultraviolet laser ablation inductively coupled plasma mass spectrometry [J ] . Geostand. Newsl. ,1998 ,22 (1) :47 -55. [14] E K Shibuya , E S Sarkis , J Enzweiler , et al.Determination of platinum group elements and gold in geological materials using an ultraviolet laser ablation high2resolution inductively coupled plasma mass spectrometric technique [J ] . J .Anal. At . Spectrom. ,1998 ,13 (8) :941 - 962. [15] L Chunsheng , Chifang Chai , Xueying Mao ,etal. Chemical speciation study of platiun group elements in geological samples by stepwise dissolution and inductively coupled plasma mass spectrometry [J ] . Anal. Chim. Acta , 1998 , 374(1) :93 - 98. [16] 段玉然,李维华. 螯合树脂富集- 激光气化等离子体发射光谱测定地质样品中的铂族元素和金 [J] .分析化学,1994 ,22 (4) :366 - 369. [17] 秦永超,江祖成. 螯合树脂静态富集/ 电热蒸发( ETV) - ICP - AES 测定铂族元素Pt 、Pd、Au [J ] . 分析试验室,1997 ,16 (4) :5 - 8. [18]张丽娟,赵丽巍. 流动注射在线清洗MPT -AES 测定铂钯金的研究 [J ] . 光谱学与光谱分析,2001 ,21 (1) :62 - 65. [19] R J Brown , W R Biggs. Determination of platinum and palladium in geological samples by Ion- Exchange Chromatography with inductivelycoupled plasma - Atomic Emission Spectrometry [J ] . Anal. chem. ,1984 , 56 :646 - 649. |
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