收稿日期: 2014-03-17
修回日期: 2014-06-03
网络出版日期: 2015-01-22
Determination of Gold in Gold Mud by Iodimetry Method
Received date: 2014-03-17
Revised date: 2014-06-03
Online published: 2015-01-22
曹文丽 , 张大勐 , 邢宁宁 . 碘量法测定金泥中的金[J]. 黄金科学技术, 2014 , 22(5) : 88 -90 . DOI: 10.11872/j.issn.1005-2518.2014.05.088
The determination of gold in gold mud by activated carbon absorption and iodimetry method was carried out.The gold mud was dissolved by aqua regia and ashed after activated carbon absorption,and then the gold was measured by Na2S2O3 titration.The optimum analytical conditions were ascertained.In this paper,the main analytical conditions such as the addition of activated carbon,speed of filtration,addition of KI,temperature and uniformity of samples were discussed on the effect of gold analysis.Gold mud was used for addition recovery tests by the method,the recoveries for gold were in the range of 97%~108%.The relative standard deviation of the sample determination results(RSD,n=6)were less than 0.50%.The analysis results in cyanidation gold mud between 10% and 30% were consistent with fire assay weight method.The method is suitable for gold in gold mud in range of 10%~30%,and has the advantage of quick,accurate,low cost and low pollution.
Key words: activated carbon; gold content; gold mud; idometry method
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